SULFATE TEST KIT
- Part number
- RXSOL-62-6198-001
- Category
- Test Kit For Water
- Brand
- RXSOL
Overview
Turbidimetric Photometric Method (0-50ppm)
Principle / Concept
This method is based on the precipitation of sulfate ion in a hydrochloric acid medium with barium chloride in such a manner as to form barium sulfate crystals of uniform size. The glycerol sulfate solution is used to maintain proper crystal size, and control of the stirring and waiting times is necessary to obtain reproducible result. The resultant turbidity is measured at a wavelength sensitive to turbidity on a photometer. The blank serves to partially cancel out interferences due to color and suspended matter.
Apparatus Required :::
Filter photometer complete with assorted laboratory glassware. ::: RXSOL-62-6198-001 doesn't include this apparatus
Chemicals Required
Glycerol Sulfate Solution ::: Part No. RXSOL-62-6198-002 http://rxmarine.com/Glycerol-Sulfate-Solution
Barium Chloride (Natural ) Solution ::: Part No. RXSOL-60-6263-250 rxmarine.com/Barium-Chloride-Solution
Sulfate Standard ::: Part No. RXSOL-62-6198-003 http://rxmarine.com/Sulfate-Standard-Solution
Applications
This procedure uses a wavelength of 420 nm and a cell with a light path of approximately 10-mm. First prepare a calibration curve for the photometer using successive dilutions of the sulfate standard to adequately cover the range of sulfate in the samples to be tested. The dilutions of the standard should be treated in exactly the same manner as that shown below for analysis of the water samples. Using a 50-ml plastic graduate, add 50 ml of sample to a 125-ml glass flask. Pipet 10 ml of glycerol sulfate solution into the flask and swirl the solution. Pipet 5 ml of distilled water into the flask, swirl the solution and use this solution to set the photometer at zero absorbance. Discard the solution and rinse the flask with distilled water. Into a second 50-ml sample, pipet 10 ml of glycerol sulfate solution and swirl. Adjust the temperature of the sample to 70 to 75F, and pipet 5 ml of neutral barium chloride solution into the same flask. Stir the solution by rotating a rubber paddle between the palms at moderate speed for exactly five seconds. Wait exactly five minutes, and then measure the absorbance on the photometer.
Calculation of Results The sulfate concentration in parts per million as SO4 is obtained by reference to the prepared sulfate calibration curve.
Limitations of Test
Color or large amounts of suspended matter will interfere with this method, but some suspended matter may be removed by filtration. Also the presence of color and suspended matter is compensated for to some extent by the blank determination. Silica in excess of 500 ppm will interfere, and in samples containing large amounts of organic material, it may not be possible to precipitate barium sulfate satisfactorily.
Characteristics and notes
Water Testing Procedures Manual ( Full Range Lab testing Methods with standard composition ratio Of Reagents ::: Available with us at 2700 INR or 54 US$ or 207 AED
SULFATE TEST
The principal problem potential posed by sulfate ions in water is the possibility of calcium sulfate scale formation. Precipitation of calcium sulfate can occur when high concentrations of both calcium and sulfate exist simultaneously. There are three primary areas of water treatment in which calcium sulfate precipitation may occur boilers, cooling systems, and ion exchangers operating in the hydrogen or acid mode.
In boilers, calcium sulfate scale formation has been reduced to a minimum by modern treatment practices. The low hardness levels largely preclude calcium sulfate boiler scale. By contrast, cooling systems are subject to calcium sulfate scale deposition because the makeup is usually not treated for hardness removal. Cooling water is usually treated with sulfuric acid for pH control, and the makeup is cycled, i.e. concentrated. Calcium sulfate scale deposition can result unless the cycles of concentration are properly controlled in conjunction with the proper use of scale control chemicals. Cation ion exchangers regenerated with sulfuric acid also can pose a major calcium sulfate problem. Calcium sulfate precipitation can be avoided by controlling the acid concentration and the flow rate through the exchanger.
Safety and SDS
Read the safety data sheet before handling. Wear suitable gloves and eye protection.
View safety data sheet
| Product Name | RXSOL-60-6198-500 |
| Product Type | Sulfate Indicator Solution |
Company Details:
RX MARINE INTERNATIONAL
105, A wing , BSEL , TECH PARK.
VASHI ,NEW BOMBAY 400703 INDIA
| Phone | +91 22 65113333 / 5555 / 9999 |
| Fax | +91 22 2781 1318 :::AOH :0091 9821214367 |
| rxsolchemicals@gmail.com |
| SARA 313 Component | CAS Number | Percent Comp. |
Dimension |
Exposure Limits |
| Barium Chloride | CAS# 10326- 27-9 | 9 -10 | W/V |
OSHA PEL 0.89 mg/mƒ |
| Hydrochloric Acid | CAS# 7647-01-0 | 1 - 6% | V/V |
OSHA PEL (C) 5 ppm, (C) 7 mg/mƒ |
| Water, Deionized ASTM Type II | CAS# 7732-18-5 | 85-96% | V/V |
None Established |
May cause irritation and burns. May be harmful if swallowed. Avoid breathing vapor or dust. Use with adequate ventilation. Avoid contact with eyes, skin, and clothes. Wash thoroughly after handling. Keep container closed.
Emergency Overview:Ingestion may Cause Gastronintestinal Disturbances. May Cause Eye
Irritation, Redness and Pain.
Inhalation:Not Expected to Be a Health Hazard.
Ingestion:Large Oral Doses may Cause Gastrointestinal Disturbances.
Skin:No Adverse Effects Expected.
Eye Contact:May Cause Irritation, Redness and Pain.
Chronic Exposure:No Information Found.
Aggravated by Exposure:No Information Found.
May cause irritation and burns. May be harmful if swallowed. Avoid breathing vapor or dust. Use with adequate ventilation. Avoid contact with eyes, skin, and clothes. Wash thoroughly after handling. Keep container closed.
|
SKIN: |
Remove contaminated clothing. Wash exposed area with soap and water. if irritation persists, seek medical attention. |
| EYES: |
Wash eyes with plenty of water for at least 15 minutes, lifting lids occasionally. Seek Medical Aid. INHALATION: Remove to fresh air. If not breathing, give artificial respiration. If breathing is difficult, give oxygen |
| INGESTION: | Give several glasses of milk or water. Vomiting may occur spontaneously, but DO NOT INDUCE! Never give anything by mouth to an unconscious person. |
|
Fire Extinguisher Type: |
Any means suitable for extinguishing |
| Fire / Explosion Hazards: | None |
| Fire Fighting Procedure: | Wear self-contained breathing apparatus and protective clothing to prevent contact with skin and clothing. |
Absorb spill with inert material, then place in a chemical waste container. Neutralize with a weak base.
Ventilate area of leak or spill. Wear appropriate personal protective equipment as specified in Section 8. Spills: Contain and Recover Liquid when Possible
Store in a cool dry place. Do not get in eyes, on skin, on clothing. Wash thoroughly after handling. Keep out of direct sunlight, away from heat, water and incompatible materials. Containers may be
|
Respiratory Protection |
None required |
| Ventilation | Local |
| OTHER | Mechanical |
| Protective Gloves | Wear appropriate gloves to prevent skin exposure |
| EYE PROTECTION | Splash Goggles |
| Other Protective Equipment |
Wear appropriate clothing to prevent skin exposure |
| BOILING POINT | Information not available |
| VAPOR PRESSURE | Information not available |
| MELTING POINT | Information not available |
| VAPOR DENSITY | Information not available |
| EVAPORATION RATE | Information not available |
| Appearance /Odors | Clear colorless liquid/no |
| Flash Point | Information not available |
| Specific Gravity | hazardous when empty. odor ~ 1 |
| Percent Volatile by | >99% |
| Evaporation Standard | |
| Auto Ignition Temp |
Not applicable |
| Lower Flamm. Limit in Air |
Not applicable |
| Upper Flamm. Limit in Air |
Not applicable |
| Solubility in Water | Soluble |
|
STABILITY |
Stable |
|
CONDITIONS TO AVOID |
Avoid Light |
|
MATERIALS TO AVOID |
Halides, ammonia, phosphates, bases |
|
HAZARDOUS DECOMPOSITION PRODUCTS |
HCL Fumes, Chlorine |
|
HAZARDOUS POLYMERIZATION |
Will Not Occur |
| Conditions to Avoid | None known |
Carcinogenic References: Hydrogen Chloride - IARC Category 3, NTP Carcinogen - Known:
No
Environmental Fate: When Released into the Soil, this Material is Not Expected to Biodegrade.
When Released into the Soil, this Material may Leach into Groundwater.
Dilute with Water and Flush to Sewer if Local Ordinances Allow, Otherwise, Whatever Cannot be Saved for Recovery or Recycling should be Managed in an Appropriate and Approved Waste
Disposal Facility. Processing, Use or Contamination of this Product may Change the Waste Management Options. State and Local Disposal Regulations May Differ from Federal Disposal Regulations. Dispose of Container and Unused Contents in Accordance with Federal, State and Local Requirements.
DOT Classification: UN1789, Hydrochloric Acid Solution, 8, PG III
DOT Regulations may change from time to time. Please consult the most recent D.O.T. regulations.
Chemical Inventory Status –
Part 1:Ingrdient
Barium Chloride (10361-37-2)
Hydrogen Chloride (7647-01-0)
TSCA Yes YES
EC Yes YES
Japan YES YES
Australia Yes YES
Chemical Inventory Status –
Part 2:Ingredient
Barium Chloride (10361-37-2)
Hydrogen Chloride (7647-01-0)
Korea Yes YES
DSL Yes YES
NDSL No NO
Phil. Yes YES
Federal, State & International Regulations –
Part 1: Ingredient.
Barium Chloride (10361-37-2)
Hydrogen Chloride (7647-01-0)
RQ No 5000
TPQ No 500
List NO YES
Chemical Catg: BARIUM COMP No
Federal, State &
International Regulations –
Part 2:Ingredient
Barium Chloride (10361-37-2)
Hydrogen Chloride (7647-01-0)
CERCLA NO 5000
261.33 No NO
8(d) No NO
Chemical Weapons Convention: No
TSCA 12 (b):No
Overexposure symtoms: Corrosive effects.: Acute-Irritation possible to skin, eyes, lungs, mucous membranes, and GI tract. Chronic- none known. Conditions aggravated/Target organs: Persons with preexisting skin, eye, or respiratory disorders may be more susceptible. May be Toxic by ingestion. Ingestion may cause severe abdominal pain, violent purging with bloody stool, confusion, paralysis, For eye contact, flush with plenty of water for
Flammability
Health Reactivity
|
Revisions |
NFPA |
| 7/30/2010 |
0.1 updated msds to 16 section from 10 section msds. STN |
| 0 |
The information herein is believed to be accurate and is offered in good faith for the user's consideration and investigation. No warranty either expressed or implied is made for the completeness or accuracy of the information whether originating from the above mentioned company or not. Users of this material should satisfy themselves by independent investigation of current scientific and medical knowledge that the material
DISCLAIMER OF LIABILITY :The information in this SDS was obtained from sources which we believe are reliable. However, the information is provided without any warranty, express or implied, regarding its correctness. The conditions or methods of handling, storage, use or disposal of the product are beyond our control and may be beyond our knowledge. For this and other reasons, we do not assume responsibility and expressly disclaim liability for loss, damage or expense arising out of or in any way connected with the handling, storage, use or disposal of the product. This MSDS was prepared and is to be used only for this product. If the product is used as a component in another product, this MSDS information may not be applicable.
Availability
SULFATE TEST KIT manufacturer supplier distributor in Mumbai, Kandla, Kolkata, Vizag, Chennai, India, Fujairah, Dubai, Sharjah, UAE, Gulf, Middle East, Muscat Oman, Kenya Africa. Get the best quality of SULFATE TEST KIT at a competitive price from us. We have ready stock of SULFATE TEST KIT in India, UAE Gulf, Oman, Kenya Africa. Contact us for bulk as well as small orders.
